Date of Defense

9-4-2026 4:30 PM

Location

F1-1077

Document Type

Dissertation Defense

Degree Name

Doctor of Philosophy in Chemical Engineering

College

COE

Department

Chemical and Petroleum Engineering

First Advisor

Prof. Basim Abu-Jdayil

Keywords

Thermal Insulators, Cellulose Aerogels, Wood Foams, Biopolymers, Green Building Materials.

Abstract

This dissertation is concerned with the use of date palm waste for the preparation of green lightweight aerogels and foams. Cellulose extracted from date palm wood waste is utilized to fabricate cellulose aerogels. Moreover, wood foams are prepared from whole biomass wood waste, without any prior treatment or extraction processes. The aim of this research is to produce sustainable, green, environmentally friendly heat insulation materials the construction, to replace commercial and fossil-fuel derived heat insulators. In this research, cellulose is extracted from date palm trees waste using both traditional and green environmentally friendly solvents. After extraction, cellulose aerogels are prepared through dissolving the cellulose in ionic liquids, a non-toxic green solvent. In addition, wood foams were prepared from whole biomass waste, without any prior treatment or extraction, using two types of biopolymer gums, which are Gellan and Xanthan gum, as binding materials. Relevant properties for the application such as thermal conductivity, thermal stability, density, porosity, water retention, and mechanical strength were evaluated. The developed material achieved high thermal insulation through low thermal conductivity values, ranging between 0.019 W/m·K to 0.074 W/m·K, for the Gellan gum wood foams, and cellulose aerogels, respectively. Moreover, the developed materials are ultralight, possessing density values as low as 31 Kg/m3, which is attributed to Xanthan gum wood foams, and sustaining high sound insulation properties, with sound absorption as high as 0.97 for cellulose aerogels. Overall, Gellan gum foams outperformed other three systems, by achieving the lowest thermal conductivity, and maintaining the second highest mechanical integrity. The developed materials hold the significance of being totally sustainable, by consisting of biomaterials, and processed through green and environmentally friendly methods. The research provides insight about the possibility of using biomaterials derived from date palm trees to produce thermal insulation in construction, whether in raw form, or through the extracted cellulose.

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Apr 9th, 4:30 PM

SUSTAINABLE CELLULOSE AEROGELS AND BIOFAOMS FROM DATE PALM WASTE FOR THERMAL INSULATION APPLICATION

F1-1077

This dissertation is concerned with the use of date palm waste for the preparation of green lightweight aerogels and foams. Cellulose extracted from date palm wood waste is utilized to fabricate cellulose aerogels. Moreover, wood foams are prepared from whole biomass wood waste, without any prior treatment or extraction processes. The aim of this research is to produce sustainable, green, environmentally friendly heat insulation materials the construction, to replace commercial and fossil-fuel derived heat insulators. In this research, cellulose is extracted from date palm trees waste using both traditional and green environmentally friendly solvents. After extraction, cellulose aerogels are prepared through dissolving the cellulose in ionic liquids, a non-toxic green solvent. In addition, wood foams were prepared from whole biomass waste, without any prior treatment or extraction, using two types of biopolymer gums, which are Gellan and Xanthan gum, as binding materials. Relevant properties for the application such as thermal conductivity, thermal stability, density, porosity, water retention, and mechanical strength were evaluated. The developed material achieved high thermal insulation through low thermal conductivity values, ranging between 0.019 W/m·K to 0.074 W/m·K, for the Gellan gum wood foams, and cellulose aerogels, respectively. Moreover, the developed materials are ultralight, possessing density values as low as 31 Kg/m3, which is attributed to Xanthan gum wood foams, and sustaining high sound insulation properties, with sound absorption as high as 0.97 for cellulose aerogels. Overall, Gellan gum foams outperformed other three systems, by achieving the lowest thermal conductivity, and maintaining the second highest mechanical integrity. The developed materials hold the significance of being totally sustainable, by consisting of biomaterials, and processed through green and environmentally friendly methods. The research provides insight about the possibility of using biomaterials derived from date palm trees to produce thermal insulation in construction, whether in raw form, or through the extracted cellulose.